Billcypher

April 5, 2020 5:16 pm

I’m very excited to be apart of this community and share my studies with you all and learn from you all. My current project is the research of piper auritum as a more environmentally friendly sourcing... View More

10 people like this.

BeeTwenty1

Idk what any of this means but I like it! Sounds interesting and out of my league. Good luck glad you’re here ✌️

Like 2 April 6, 2020

Ryan

Thats sounds super interesting cant wait to here more! Also nice to see another gravity falls fan

Like 1 April 6, 2020

Admin

May 4, 2023 2:54 pm Official DMT World

Billcypher shared a photo

April 5, 2020 4:56 pm

Good morning everyone. I’d like to talk about the synthesis of ammonium chloride with otc chemicals. Those of you interested in the synthesis of MethylAmine, mdma and the likes may find this informati... View More

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4/25

crashedfx

And 5meo synthesis has been described in Shulgin's book, it just seems way too complicated to me LOL "To a cooled and well-stirred solution of 16 g 5-methoxyindole in 200 mL anhydrous Et2O there was added, dropwise, 25 g oxalyl chloride. Stirring was continued for an additional 10 min, then the red... View MoreAnd 5meo synthesis has been described in Shulgin's book, it just seems way too complicated to me LOL "To a cooled and well-stirred solution of 16 g 5-methoxyindole in 200 mL anhydrous Et2O there was added, dropwise, 25 g oxalyl chloride. Stirring was continued for an additional 10 min, then the red solids were removed by filtration, washed lightly with Et2O, and returned to the reaction beaker as a suspension in 200 mL fresh anhydrous Et2O. To this there was added a solution of 8.5 g dimethylamine in 25 mL anhydrous Et2O which discharged the red color. Stirring was continued for an additional 0.5 h, and the solids were removed by filtration and washed with Et2O. These were suspended in H2O, filtered, and washed alternately with H2O and Et2O. Recrystallization from THF / Et2O provided 20 g (75%) 5-methoxy-N,N-dimethylindol-3-ylglyoxylamide, mp 223-223.5 °C, as fine white crystals. To a well-stirred suspension of 11.7 g LAH in 350 mL anhydrous Et2O there was added, in small portions, a suspension of 18.5 g 5-methoxy-N,N-dimethylindol-3-ylglyoxylamide in 200 mL hot benzene. The last of the solids were rinsed in with anhydrous Et2O and the mixture held at reflux for 1.5 h. After cooling with an external ice bath, the reaction complex and excess hydride were decomposed by the cautious addition of H2O. The inorganic solids were removed by filtration, the filter cake washed with additional Et2O, the filtrate and washing were combined and dried over anhydrous MgSO4, and the solvents removed under vacuum. The residue was distilled at the KugelRohr to provide a colorless fraction distilling at 160-170 °C at 0.6 mm/Hg, that crystallized on cooling. There was thus obtained 12.8 g (78%) 5-methoxy-N,N-dimethyltryptamine (5-MeO-DMT) which on recrystallization from hexane had a mp 69-70 °C. The hydrochloride salt can be made by passing a stream of hydrogen chloride gas through an Et2O solution of the base. It, upon recrystallization from EtOH / Et2O, had a mp of 145-146 °C."

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Like 1 April 6, 2020

Billcypher

Crashedfx. You’d probably know better than I Would On the matte, it sounds like you’ve studied it a lot. What Im talking about though is the only synthetic dmt I tried was n-dmt or some kind of variant and I noticed a significant difference in the trip it produced compared to what was taken from the... View More

Like April 6, 2020

invitroHulk

5meo and NNdmt are different some plants do contain 5meo.. mhrb bark is NN DMT.. how many hours does it take to synthesize MDMA and what’s the cost for chemicals

Like 1 April 6, 2020