Good morning everyone. I’d like to talk about the synthesis of ammonium chloride with otc chemicals. Those of you interested in the synthesis of MethylAmine, mdma and the likes may find this information useful. Some of you may have watched Nile red on YouTube attempt and fail to make ammonium chloride. So this is me telling you guys how it’s done successfully. 300ml ammonia hydroxide solution is added to 300ml hydrochloric acid solution . The ammonia hydroxide solution should contain 10% ammonia and the hydrochloric acid solution should contain 20% hydrochloric acid. Ammonium chloride gas will start to come in some nice white clouds out of the beaker. You’ll notice an exothermic reaction occurs. We then transfer our beaker to our hot plate on high and bring it to a boil. We will then boil off or evaporate 3/4 of the solution. So there should be 150ml of liquid left in the beaker. This is then removed from the hot plate and slow cooled. After it’s at room temp I transfer the beaker to an ice bath and ammonium chloride crystals form in solution. The solution is then poured into a Büchner funnel under vaccum to separate the ammonium chloride crystals from solution. We let the crystals dry in the funnel and then we have reagent grade ammonium chloride. If your initial solutions used were free of impurity. You can further clean end product with a chilled ammonia hydroxide wash if necessary. I hope this helps those learning to synthesis mdma. One less thing you will have to get from your chem suppliers and can just make yourself under the radar. God bless all of you taking on the challenge of synthesizing mdma domestically. The dea has made some major hurdles for us to jump but we will always succeed in our mission of bringing love and unity to our communities if we are dedicated enough. I hope this helps some young aspiring chemist.
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crashedfx
And 5meo synthesis has been described in Shulgin's book, it just seems way too complicated to me LOL
"To a cooled and well-stirred solution of 16 g 5-methoxyindole in 200 mL anhydrous Et2O there was added, dropwise, 25 g oxalyl chloride. Stirring was continued for an additional 10 min, then the red... View More
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April 6, 2020

Billcypher
Crashedfx. You’d probably know better than I Would On the matte, it sounds like you’ve studied it a lot. What Im talking about though is the only synthetic dmt I tried was n-dmt or some kind of variant and I noticed a significant difference in the trip it produced compared to what was taken from the... View More
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April 6, 2020

invitroHulk
5meo and NNdmt are different some plants do contain 5meo.. mhrb bark is NN DMT.. how many hours does it take to synthesize MDMA and what’s the cost for chemicals
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April 6, 2020

Billcypher
Thanks for the info invitrohulk. sounds like I need to do a lot of home work on dmt. I’ll make a thread tonight talking about the bright star synth.
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April 6, 2020