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Matty580

Male. Lives in out beyond the green glow where all things become one, United States. Born on June 8, 1900. Is single.

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I'm just an old man that lives by a set of very simple principles. I've been to the edge and beyond ... View More

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Matty580

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Matty580

November 17, 2024 6:47 pm

ok so who has tried separating 5-meo from N,N Dmt using swims method with anhydrous acetone and anhyrous acetone citric acid solution

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HappyKB

I have not, but if you try let us know how it goes.

Like November 18, 2024

Matty580

ok HappyKB ive tried it and very strange things are in the making im trying another round 2nite with a more scientific approach so followed to the letter I baked a nice thin layer of epsom salt( magnesium sulfate) in the oven for three hours at 225 degrees I found that the 200 degrees in the tek did... View Moreok HappyKB ive tried it and very strange things are in the making im trying another round 2nite with a more scientific approach so followed to the letter I baked a nice thin layer of epsom salt( magnesium sulfate) in the oven for three hours at 225 degrees I found that the 200 degrees in the tek didn't work the best where im at like I said before teks are great but there's variables not mentioned that can play hell on reactions ambient temperature, quality of reagents, humidity hell even altitude but I know the first step worked once you bake the epsom salt you can totally see a change in it's makeup it's much more white and very dry looking, you have to work fast as it starts wicking moisture from the air almost immediately I filled three quart mason jars 1/3 full of the prepared salt and then filled the jars with acetone and put them in the freezer for 48hrs. I know this step worked as well all the epsome salt was now in big hard chunks.i quickly poured the now anhydrous acetone into new jars all but 16oz Wirth this went into a separate jar that I added citric acid to I put a bunch of dmt that had been already totally prepared it was really nice looking crystals yellow but nice. I know someone's gonna say it's yellow because I didn't defat it. Cybs hybrid salt tek doesn't recommend it especially with mhrb with acacia bark id recommended it.Mines usually yellow because I recycle my naptha all the time ill use new if I'm recrystallizing. But anywho the dmt immediately resolved in the acetone, I then added the acetone/ citric acid solution and was hopeful to see maybe something even grain of sand size piece oh hell no everything dropped out of the solution and it's quite the crazy looking reaction foams a bunch and this big whitish blob starts growing I kept adding the citric acid solution as instructed eventually the reaction stops the acetone goes clear well yellow but clear it's cloudy as all get out when things are happening and the big white blob was now a slightly smaller dark as hell yellow blob with the consistency of soft candle wax I assumed all fat I poured off the acetone as per the tek any N,N dmt should all be in that. Your supposed to evaporate it and your left with dmt citrate no problem you basify it and you got ur freebase again ive worked with acetone for years it evaps real quick ive had a fan on it for 2 days its still not totally evaded and now has the consistency of yellow snot, but that's not what's messed up I actually had to sit down and twist up a doobie and ponder this that waxy yellow blob was indestructible I tried fresh naptha that was heated nothing dented it except industrial grade distilled white vinegar which is 30% acidity it will burn you as bad as muriatic acid maybe worse it took a lot of shaking the jar but it all dissolved here's where it got a little crazy I decided to drop in sodium carbonate solution with a ph at least 9.5 probably a little higher make sure you have it in a very tall vessel because the reaction is out of control foaming and bubbling it was pissed off I kept adding until the ph in the solution hit 9.5 at this point the reaction dyes and the solution losses all vinegar smell and industrial grade is very strong smelling I then added clean naptha 50ml worth it jumped from the sodium carbonate solution to the naphtha instantly there was a very fine layer of contaminate on the bottom of the jar and also a very thin layer of cloudy funk separating the 2 I pulled the naptha off started freeze precipitation not thinking much would come of it I got home from work 2day that container is full of totally pure white crystals from hell so im still at a total lose on this one please for God's sake someone give me some feed back I know if I took the time to reseach I could probably find the answer but I'm on another ok im on 2 other missions 1st I'm preparing for tekking some cactus powder for the first time and I'm also getting ready to tek some boomers into crystal but right now I just need to hear from the veterans that have forgotten more about trekking dmt then ill probably ever know L.L.R.

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Like 1 November 19, 2024

Matty580

hers the yellow blob this is a small one I'm doing a weight comparison from start to finish ill let you know the results

Like 1 November 19, 2024

HappyKB

Very interesting and informative thank you I'm interested to hear more to see what comes.

Like November 19, 2024

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